Structures by: Färber C.

Total: 62

C43H60Fe2N4O

C43H60Fe2N4O

Siemeling, UlrichFärber, ChristianBruhn, ClemensLeibold, MichaelSelent, DetlefBaumann, Wolfgangvon Hopffgarten, MoritzGoedecke, CatharinaFrenking, Gernot

Chemical Science (2010) 1, 6 697

a=16.3194(13)Å   b=10.7454(5)Å   c=22.9601(17)Å

α=90.00°   β=97.397(6)°   γ=90.00°

C26H39FeN3

C26H39FeN3

Siemeling, UlrichFärber, ChristianBruhn, ClemensLeibold, MichaelSelent, DetlefBaumann, Wolfgangvon Hopffgarten, MoritzGoedecke, CatharinaFrenking, Gernot

Chemical Science (2010) 1, 6 697

a=15.253(2)Å   b=9.8425(17)Å   c=16.706(2)Å

α=90.00°   β=95.195(11)°   γ=90.00°

C25H36FeN2O2

C25H36FeN2O2

Siemeling, UlrichFärber, ChristianBruhn, ClemensLeibold, MichaelSelent, DetlefBaumann, Wolfgangvon Hopffgarten, MoritzGoedecke, CatharinaFrenking, Gernot

Chemical Science (2010) 1, 6 697

a=12.1007(16)Å   b=17.090(2)Å   c=11.5086(13)Å

α=90.00°   β=97.616(10)°   γ=90.00°

C32H16F20N2O2Sr

C32H16F20N2O2Sr

Fischer, Christian A.Rösch, AndreasElsen, HolgerBallmann, GerdWiesinger, MichaelLanger, JensFärber, ChristianHarder, Sjoerd

Dalton transactions (Cambridge, England : 2003) (2019) 48, 20 6757-6766

a=15.8863(2)Å   b=12.46800(10)Å   c=17.3641(2)Å

α=90°   β=107.9700(10)°   γ=90°

C32H16F20MgN2O2

C32H16F20MgN2O2

Fischer, Christian A.Rösch, AndreasElsen, HolgerBallmann, GerdWiesinger, MichaelLanger, JensFärber, ChristianHarder, Sjoerd

Dalton transactions (Cambridge, England : 2003) (2019) 48, 20 6757-6766

a=9.2647(4)Å   b=20.2362(8)Å   c=17.7948(7)Å

α=90°   β=100.799(5)°   γ=90°

C32H16CaF20N2O2

C32H16CaF20N2O2

Fischer, Christian A.Rösch, AndreasElsen, HolgerBallmann, GerdWiesinger, MichaelLanger, JensFärber, ChristianHarder, Sjoerd

Dalton transactions (Cambridge, England : 2003) (2019) 48, 20 6757-6766

a=9.2667(2)Å   b=20.4436(4)Å   c=17.8288(4)Å

α=90°   β=98.013(2)°   γ=90°

C36H36F20Mg2N4Si4

C36H36F20Mg2N4Si4

Fischer, Christian A.Rösch, AndreasElsen, HolgerBallmann, GerdWiesinger, MichaelLanger, JensFärber, ChristianHarder, Sjoerd

Dalton transactions (Cambridge, England : 2003) (2019) 48, 20 6757-6766

a=11.7023(3)Å   b=15.6263(3)Å   c=13.0643(3)Å

α=90°   β=111.787(3)°   γ=90°

C32H20F20MgN2O2

C32H20F20MgN2O2

Fischer, Christian A.Rösch, AndreasElsen, HolgerBallmann, GerdWiesinger, MichaelLanger, JensFärber, ChristianHarder, Sjoerd

Dalton transactions (Cambridge, England : 2003) (2019) 48, 20 6757-6766

a=28.9330(3)Å   b=10.43410(10)Å   c=11.29390(10)Å

α=90°   β=90°   γ=90°

C36H36Ca2F20N4Si4

C36H36Ca2F20N4Si4

Fischer, Christian A.Rösch, AndreasElsen, HolgerBallmann, GerdWiesinger, MichaelLanger, JensFärber, ChristianHarder, Sjoerd

Dalton transactions (Cambridge, England : 2003) (2019) 48, 20 6757-6766

a=8.8864(2)Å   b=24.4425(6)Å   c=24.5767(7)Å

α=63.347(3)°   β=83.970(2)°   γ=89.760(2)°

C32H20CaF20N2O2

C32H20CaF20N2O2

Fischer, Christian A.Rösch, AndreasElsen, HolgerBallmann, GerdWiesinger, MichaelLanger, JensFärber, ChristianHarder, Sjoerd

Dalton transactions (Cambridge, England : 2003) (2019) 48, 20 6757-6766

a=9.2631(3)Å   b=20.3100(4)Å   c=18.1174(4)Å

α=90°   β=91.034(2)°   γ=90°

0.25(C144H144F80N16Si16Sr8),2(C6H6)

0.25(C144H144F80N16Si16Sr8),2(C6H6)

Fischer, Christian A.Rösch, AndreasElsen, HolgerBallmann, GerdWiesinger, MichaelLanger, JensFärber, ChristianHarder, Sjoerd

Dalton transactions (Cambridge, England : 2003) (2019) 48, 20 6757-6766

a=12.5188(2)Å   b=20.5028(3)Å   c=23.2272(2)Å

α=99.6880(10)°   β=99.7680(10)°   γ=102.2650(10)°

C40H70CaN4OSi2

C40H70CaN4OSi2

Causero, AndreaBallmann, GerdPahl, JürgenFärber, ChristianIntemann, JuliaHarder, Sjoerd

Dalton transactions (Cambridge, England : 2003) (2017) 46, 6 1822-1831

a=11.30050(10)Å   b=20.2024(2)Å   c=39.1907(2)Å

α=102.3440(10)°   β=90.1900(10)°   γ=90.3460(10)°

C32H48CaN3

C32H48CaN3

Causero, AndreaBallmann, GerdPahl, JürgenFärber, ChristianIntemann, JuliaHarder, Sjoerd

Dalton transactions (Cambridge, England : 2003) (2017) 46, 6 1822-1831

a=8.88056(13)Å   b=15.1230(2)Å   c=22.2473(3)Å

α=90°   β=96.5639(13)°   γ=90°

C62H92Ca2N4O2,C6H6

C62H92Ca2N4O2,C6H6

Causero, AndreaBallmann, GerdPahl, JürgenFärber, ChristianIntemann, JuliaHarder, Sjoerd

Dalton transactions (Cambridge, England : 2003) (2017) 46, 6 1822-1831

a=13.3510(5)Å   b=16.3688(6)Å   c=15.0996(5)Å

α=90°   β=100.888(3)°   γ=90°

C66H104Ca2N4O2

C66H104Ca2N4O2

Causero, AndreaBallmann, GerdPahl, JürgenFärber, ChristianIntemann, JuliaHarder, Sjoerd

Dalton transactions (Cambridge, England : 2003) (2017) 46, 6 1822-1831

a=11.98073(15)Å   b=15.11446(17)Å   c=18.0466(2)Å

α=90°   β=97.5028(12)°   γ=90°

C62H92Ca2N4O2

C62H92Ca2N4O2

Causero, AndreaBallmann, GerdPahl, JürgenFärber, ChristianIntemann, JuliaHarder, Sjoerd

Dalton transactions (Cambridge, England : 2003) (2017) 46, 6 1822-1831

a=12.2642(3)Å   b=15.2818(3)Å   c=16.5278(3)Å

α=90°   β=103.457(2)°   γ=90°

C68H106Ca2N6O2

C68H106Ca2N6O2

Causero, AndreaBallmann, GerdPahl, JürgenFärber, ChristianIntemann, JuliaHarder, Sjoerd

Dalton transactions (Cambridge, England : 2003) (2017) 46, 6 1822-1831

a=14.4825(2)Å   b=13.02210(10)Å   c=18.2443(2)Å

α=90°   β=100.2860(10)°   γ=90°

C39H69CaN3O2Si2,C3H3

C39H69CaN3O2Si2,C3H3

Causero, AndreaBallmann, GerdPahl, JürgenFärber, ChristianIntemann, JuliaHarder, Sjoerd

Dalton transactions (Cambridge, England : 2003) (2017) 46, 6 1822-1831

a=11.68700(18)Å   b=18.0806(2)Å   c=21.8110(4)Å

α=90°   β=105.3719(17)°   γ=90°

C22H20FeP2

C22H20FeP2

Hitzel, SandraFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton Trans. (2017)

a=5.9967(14)Å   b=26.083(7)Å   c=11.900(4)Å

α=90°   β=101.87(2)°   γ=90°

C26H16F12FeP2

C26H16F12FeP2

Hitzel, SandraFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton Trans. (2017)

a=8.9360(7)Å   b=8.1613(5)Å   c=18.0145(16)Å

α=90°   β=94.549(7)°   γ=90°

C34H50FeLi2N4P2

C34H50FeLi2N4P2

Hitzel, SandraFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton Trans. (2017)

a=10.8879(8)Å   b=12.9242(8)Å   c=14.9695(10)Å

α=101.557(5)°   β=91.535(6)°   γ=111.792(5)°

C54H46Fe2Ni3P4

C54H46Fe2Ni3P4

Hitzel, SandraFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton Trans. (2017)

a=10.126(3)Å   b=11.395(3)Å   c=12.124(3)Å

α=103.436(19)°   β=106.865(19)°   γ=115.180(18)°

C64H86Fe2Ni4O2P4

C64H86Fe2Ni4O2P4

Hitzel, SandraFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton Trans. (2017)

a=14.0188(8)Å   b=10.6198(5)Å   c=20.1658(12)Å

α=90°   β=96.178(5)°   γ=90°

(DIPP-NBN)Ca.(THF)4

C40H67BCaN2O4

Freitag, BenjaminFischer, Christian A.Penafiel, JohanneBallmann, GerdElsen, HolgerFärber, ChristianPiesik, Dirk F.Harder, Sjoerd

Dalton Trans. (2017)

a=10.1263(10)Å   b=10.1718(9)Å   c=11.2367(10)Å

α=81.148(6)°   β=66.376(6)°   γ=74.572(6)°

C36H59BMgN2O3

C36H59BMgN2O3

Freitag, BenjaminFischer, Christian A.Penafiel, JohanneBallmann, GerdElsen, HolgerFärber, ChristianPiesik, Dirk F.Harder, Sjoerd

Dalton Trans. (2017)

a=10.5266(2)Å   b=17.9167(3)Å   c=18.7856(4)Å

α=90°   β=90°   γ=90°

C38H50F12FeN6P2Zr2

C38H50F12FeN6P2Zr2

Hitzel, SandraFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton Trans. (2017)

a=41.181(3)Å   b=12.8318(13)Å   c=18.5900(15)Å

α=90°   β=108.288(6)°   γ=90°

C23H32FeNiP2

C23H32FeNiP2

Hitzel, SandraFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton Trans. (2017)

a=20.4381(14)Å   b=6.4522(3)Å   c=18.5152(12)Å

α=90°   β=116.319(5)°   γ=90°

C46H64Fe2Ni4O2P4,C28H36FeNi2P2,3(C6H6)

C46H64Fe2Ni4O2P4,C28H36FeNi2P2,3(C6H6)

Hitzel, SandraFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton Trans. (2017)

a=10.1479(4)Å   b=18.7714(6)Å   c=45.1642(19)Å

α=90°   β=96.353(3)°   γ=90°

C52H92Fe2Li4N4P4

C52H92Fe2Li4N4P4

Hitzel, SandraFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton Trans. (2017)

a=10.5717(9)Å   b=10.9440(9)Å   c=13.6502(10)Å

α=70.253(6)°   β=80.074(6)°   γ=89.001(7)°

C18H28FeP2

C18H28FeP2

Hitzel, SandraFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton Trans. (2017)

a=5.9610(8)Å   b=8.9856(11)Å   c=9.7083(12)Å

α=65.070(9)°   β=80.485(10)°   γ=78.753(10)°

C36H54Fe2NiP4

C36H54Fe2NiP4

Hitzel, SandraFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton Trans. (2017)

a=10.5735(6)Å   b=12.3319(7)Å   c=14.3840(8)Å

α=87.958(5)°   β=74.515(4)°   γ=87.467(5)°

C34H54FeN6P2Zr2

C34H54FeN6P2Zr2

Hitzel, SandraFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton Trans. (2017)

a=13.4517(4)Å   b=16.4468(4)Å   c=35.2138(13)Å

α=90°   β=98.545(3)°   γ=90°

C16H16FeN2

C16H16FeN2

Rittinghaus, StefanFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton transactions (Cambridge, England : 2003) (2014) 43, 9 3508-3520

a=20.082(2)Å   b=13.8650(10)Å   c=9.3820(7)Å

α=90.00°   β=90.00°   γ=90.00°

C26H35BF4FeN2

C26H35BF4FeN2

Rittinghaus, StefanFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton transactions (Cambridge, England : 2003) (2014) 43, 9 3508-3520

a=26.917(2)Å   b=13.8187(7)Å   c=17.8272(14)Å

α=90.00°   β=125.348(5)°   γ=90.00°

C30H36ClFeN2Rh

C30H36ClFeN2Rh

Rittinghaus, StefanFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton transactions (Cambridge, England : 2003) (2014) 43, 9 3508-3520

a=24.2589(15)Å   b=12.7596(4)Å   c=21.9110(14)Å

α=90.00°   β=119.247(4)°   γ=90.00°

C33H30ClFeN2O2Rh

C33H30ClFeN2O2Rh

Rittinghaus, StefanFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton transactions (Cambridge, England : 2003) (2014) 43, 9 3508-3520

a=21.200(2)Å   b=6.6361(5)Å   c=21.901(3)Å

α=90.00°   β=112.394(8)°   γ=90.00°

C24H24ClFeN2O2Rh

C24H24ClFeN2O2Rh

Rittinghaus, StefanFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton transactions (Cambridge, England : 2003) (2014) 43, 9 3508-3520

a=12.8531(8)Å   b=18.9358(7)Å   c=20.6272(11)Å

α=90.00°   β=104.753(4)°   γ=90.00°

C34H46ClFeN2Rh

C34H46ClFeN2Rh

Rittinghaus, StefanFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton transactions (Cambridge, England : 2003) (2014) 43, 9 3508-3520

a=11.7145(17)Å   b=12.8372(17)Å   c=21.686(3)Å

α=81.088(10)°   β=82.726(11)°   γ=76.040(11)°

4(C39H42ClFeN2Rh),CH2Cl2

4(C39H42ClFeN2Rh),CH2Cl2

Rittinghaus, StefanFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton transactions (Cambridge, England : 2003) (2014) 43, 9 3508-3520

a=11.6403(7)Å   b=14.8878(10)Å   c=20.1701(12)Å

α=98.297(5)°   β=91.535(5)°   γ=103.422(5)°

C31H39FeN2,CH2Cl2,BF4

C31H39FeN2,CH2Cl2,BF4

Siemeling, UlrichFärber, ChristianBruhn, Clemens

Chemical communications (Cambridge, England) (2008) 34, 1 98-100

a=7.9008(12)Å   b=18.7777(19)Å   c=10.3761(17)Å

α=90.00°   β=90.019(13)°   γ=90.00°

C39H50ClFeN2Rh

C39H50ClFeN2Rh

Siemeling, UlrichFärber, ChristianBruhn, Clemens

Chemical communications (Cambridge, England) (2008) 34, 1 98-100

a=12.8330(12)Å   b=20.430(2)Å   c=12.3078(14)Å

α=90.00°   β=90.00°   γ=90.00°

4(C31H38FeN2),C7H8

4(C31H38FeN2),C7H8

Siemeling, UlrichFärber, ChristianBruhn, Clemens

Chemical communications (Cambridge, England) (2008) 34, 1 98-100

a=10.763(3)Å   b=16.153(5)Å   c=16.339(5)Å

α=71.83(2)°   β=70.42(2)°   γ=81.36(2)°

C48F40Mg2N4

C48F40Mg2N4

Fischer, Christian A.Rösch, AndreasElsen, HolgerBallmann, GerdWiesinger, MichaelLanger, JensFärber, ChristianHarder, Sjoerd

Dalton transactions (Cambridge, England : 2003) (2019) 48, 20 6757-6766

a=10.7838(4)Å   b=10.8947(4)Å   c=11.2504(4)Å

α=90.810(3)°   β=113.380(4)°   γ=102.982(3)°

C30H58FeLi2N4P2

C30H58FeLi2N4P2

Hitzel, SandraFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton Trans. (2017)

a=21.7734(5)Å   b=13.2129(4)Å   c=24.9840(7)Å

α=90°   β=90°   γ=90°

C32H28FeNi2P2,C6H6

C32H28FeNi2P2,C6H6

Hitzel, SandraFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton Trans. (2017)

a=12.0027(4)Å   b=9.7307(4)Å   c=27.0982(8)Å

α=90°   β=90.452(2)°   γ=90°

C28H34ClFeN2O2Rh

C28H34ClFeN2O2Rh

Rittinghaus, StefanFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Dalton transactions (Cambridge, England : 2003) (2014) 43, 9 3508-3520

a=11.797(3)Å   b=19.483(3)Å   c=12.948(2)Å

α=90.00°   β=115.250(14)°   γ=90.00°

C35H38FeMoN2O4

C35H38FeMoN2O4

Siemeling, UlrichFärber, ChristianBruhn, Clemens

Chemical communications (Cambridge, England) (2008) 34, 1 98-100

a=13.549(2)Å   b=20.097(5)Å   c=11.2263(19)Å

α=90.00°   β=90.00°   γ=90.00°

C70H100Ca2N4,4(C6H6)

C70H100Ca2N4,4(C6H6)

Causero, AndreaBallmann, GerdPahl, JürgenZijlstra, HarmenFärber, ChristianHarder, Sjoerd

Organometallics (2016) 35, 19 3350

a=10.4550(2)Å   b=10.5225(2)Å   c=19.8508(3)Å

α=83.3598(15)°   β=87.9438(15)°   γ=69.2211(18)°

C41H67CaN3Si2

C41H67CaN3Si2

Causero, AndreaBallmann, GerdPahl, JürgenZijlstra, HarmenFärber, ChristianHarder, Sjoerd

Organometallics (2016) 35, 19 3350

a=9.87724(17)Å   b=12.3264(2)Å   c=33.7986(7)Å

α=90°   β=92.2021(17)°   γ=90°

C40H73CaN3OSi2

C40H73CaN3OSi2

Causero, AndreaBallmann, GerdPahl, JürgenZijlstra, HarmenFärber, ChristianHarder, Sjoerd

Organometallics (2016) 35, 19 3350

a=14.7482(7)Å   b=18.0397(7)Å   c=16.8077(7)Å

α=90°   β=94.156(5)°   γ=90°

{[tBuC(NDIPP)2]CaH}3.(Et2O)2

C95H152Ca3N6O2

Causero, AndreaBallmann, GerdPahl, JürgenZijlstra, HarmenFärber, ChristianHarder, Sjoerd

Organometallics (2016) 35, 19 3350

a=27.3042(2)Å   b=12.40850(10)Å   c=58.1368(3)Å

α=90°   β=94.4550(10)°   γ=90°

C113H166Ca3N6O2,C6H14

C113H166Ca3N6O2,C6H14

Causero, AndreaBallmann, GerdPahl, JürgenZijlstra, HarmenFärber, ChristianHarder, Sjoerd

Organometallics (2016) 35, 19 3350

a=15.1967(2)Å   b=18.2301(3)Å   c=25.8609(4)Å

α=92.8035(13)°   β=101.6317(12)°   γ=114.0730(15)°

C39H71CaN3OSi2

C39H71CaN3OSi2

Causero, AndreaBallmann, GerdPahl, JürgenZijlstra, HarmenFärber, ChristianHarder, Sjoerd

Organometallics (2016) 35, 19 3350

a=10.6373(4)Å   b=12.4259(3)Å   c=16.4223(3)Å

α=90.146(2)°   β=92.606(2)°   γ=98.163(3)°

C64H110Ca2N6Si4

C64H110Ca2N6Si4

Causero, AndreaBallmann, GerdPahl, JürgenZijlstra, HarmenFärber, ChristianHarder, Sjoerd

Organometallics (2016) 35, 19 3350

a=11.78345(19)Å   b=15.5905(2)Å   c=23.5944(4)Å

α=102.6714(13)°   β=94.2421(13)°   γ=106.0615(14)°

2(C38H59CaN3Si2),4(C7H8)

2(C38H59CaN3Si2),4(C7H8)

Causero, AndreaBallmann, GerdPahl, JürgenZijlstra, HarmenFärber, ChristianHarder, Sjoerd

Organometallics (2016) 35, 19 3350

a=16.3967(2)Å   b=16.4260(3)Å   c=21.1559(4)Å

α=110.503(2)°   β=102.6180(10)°   γ=100.0220(10)°

C50H72CaN4O

C50H72CaN4O

Causero, AndreaBallmann, GerdPahl, JürgenZijlstra, HarmenFärber, ChristianHarder, Sjoerd

Organometallics (2016) 35, 19 3350

a=12.12062(13)Å   b=16.59171(16)Å   c=22.9746(2)Å

α=90°   β=90.4699(9)°   γ=90°

C38H73CaKN4Si4

C38H73CaKN4Si4

Causero, AndreaBallmann, GerdPahl, JürgenZijlstra, HarmenFärber, ChristianHarder, Sjoerd

Organometallics (2016) 35, 19 3350

a=18.9149(2)Å   b=11.58948(14)Å   c=21.6672(3)Å

α=90°   β=99.4158(12)°   γ=90°

C56H45Cl2N4P2Ru,CH2Cl2

C56H45Cl2N4P2Ru,CH2Cl2

Hitzel, SandraFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Organometallics (2014) 33, 1 425

a=29.236(2)Å   b=14.2862(8)Å   c=12.2213(7)Å

α=90.00°   β=90.00°   γ=90.00°

C20H17N4,CH4O,Cl

C20H17N4,CH4O,Cl

Hitzel, SandraFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Organometallics (2014) 33, 1 425

a=13.6869(10)Å   b=10.0088(6)Å   c=14.2901(11)Å

α=90.00°   β=97.194(6)°   γ=90.00°

C56H44Cl2N3P2Ru

C56H44Cl2N3P2Ru

Hitzel, SandraFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Organometallics (2014) 33, 1 425

a=28.594(2)Å   b=15.4001(10)Å   c=12.3532(7)Å

α=90.00°   β=90.00°   γ=90.00°

2(C56H44ClN3P2Ru),C7H8

2(C56H44ClN3P2Ru),C7H8

Hitzel, SandraFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Organometallics (2014) 33, 1 425

a=23.5798(12)Å   b=14.0799(6)Å   c=30.4380(15)Å

α=90.00°   β=101.877(4)°   γ=90.00°

C56H45ClN4P2Ru

C56H45ClN4P2Ru

Hitzel, SandraFärber, ChristianBruhn, ClemensSiemeling, Ulrich

Organometallics (2014) 33, 1 425

a=10.8334(11)Å   b=12.9900(13)Å   c=16.6442(18)Å

α=93.013(8)°   β=91.987(8)°   γ=99.918(8)°